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Synthesis of Polydisperse Boron Carbide and Synthesis of a Ceramic on Its Basis Full article

Journal Russian Journal of Applied Chemistry
ISSN: 1070-4272
Output data Year: 2019, Volume: 92, Number: 6, Pages: 750-758 Pages count : 9 DOI: 10.1134/s1070427219060041
Tags boron carbide; chromium carbide; hot compaction; micro-hardness; nanofibrous carbon; sintering additive
Authors Krutskii Yu.L. 1 , Nepochatov Yu.K. 2 , Pel’ A.N. 1 , Skovorodin I.N. 3 , Dyukova K.D. 4 , Krutskaya T.M. 5 , Kuchumova I.D. 1 , Mats O.E. 1 , Tyurin A.G. 1 , Emurlaeva Yu.Yu. 1 , Podryabinkin S.I. 1
Affiliations
1 Novosibirsk State Technical University
2 NANOKERAMIKS
3 Institute of Automation and Electrometry
4 International Research Center on Thermal Physics and Power Engineering
5 Novosibirsk State University of Architecture and Civil Engineering

Abstract: Results obtained in a study of the process of synthesis of a polydisperse boron carbide powder (average particle size 2.10 µm) characterized by a broad particle size distribution are presented. The process in which a ceramic is produced from the thus synthesized boron carbide by hot compaction was also analyzed. In some cases, a sintering additive, highly dispersed chromium carbide powder (average particle size 7.13 µm), was used. The hot compaction was performed in argon at moderate parameters: pressure 35 MPa and temperature 1950°C. The porosity and water-absorption capacity of the samples obtained are very low and do not exceed 0.02%. The average values of the bending and compression strengths were 406 and 1553 MPa, respectively. A microhardness of about 42 GPa was reached in sintering of boron carbide. The microhardness in sintering of boron carbide with addition of chromium carbide was 45–46 GPa.
Cite: Krutskii Y.L. , Nepochatov Y.K. , Pel’ A.N. , Skovorodin I.N. , Dyukova K.D. , Krutskaya T.M. , Kuchumova I.D. , Mats O.E. , Tyurin A.G. , Emurlaeva Y.Y. , Podryabinkin S.I.
Synthesis of Polydisperse Boron Carbide and Synthesis of a Ceramic on Its Basis
Russian Journal of Applied Chemistry. 2019. V.92. N6. P.750-758. DOI: 10.1134/s1070427219060041 WOS Scopus РИНЦ OpenAlex
Identifiers:
Web of science: WOS:000479143900004
Scopus: 2-s2.0-85070237807
Elibrary: 41372144
OpenAlex: W2965714333
Citing:
DB Citing
Scopus 9
OpenAlex 8
Web of science 4
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