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Experimental evidence and possible mechanism of melt formation at the inter-particle contacts during spark plasma sintering of TiC-Cu composite particles Full article

Journal International Journal of Refractory Metals and Hard Materials
ISSN: 0263-4368
Output data Year: 2024, Volume: 122, Pages: 106732 Pages count : 1 DOI: 10.1016/j.ijrmhm.2024.106732
Tags Spark plasma sintering, Melting, Inter-particle contact, Micro-arc
Authors Dudina Dina V. 1,2 , Shtertser Alexandr A. 1 , Vidyuk Tomila M. 2,3 , Bokhonov Boris B. 2
Affiliations
1 Lavrentyev Institute of Hydrodynamics
2 Institute of Solid State Chemistry and Mechanochemistry of SB RAS
3 Khristianovich Institute of Theoretical and Applied Mechanics SB RAS

Funding (1)

1 Министерство науки и высшего образования Российской Федерации FWGG-2021-0005

Abstract: In the present work, the evidence of the melt formation at the contacts between composite TiC-Cu particles formed by high-energy ball milling was found in the microstructure of compacts obtained by spark plasma sintering at real temperatures of the sample of 725–925 ◦C. The voltage drop associated with a contact that could have been heated up to the melting point of copper was calculated to be much higher than the voltage across the whole sample during SPS. As the formation of melt could not be attributed to simple overheating of small crosssectional area contacts (bridges), another explanation of the observed effect was sought. A mechanism based on the micro-arc formation was proposed to explain the observed melt formation in the sintered composites.
Cite: Dudina D.V. , Shtertser A.A. , Vidyuk T.M. , Bokhonov B.B.
Experimental evidence and possible mechanism of melt formation at the inter-particle contacts during spark plasma sintering of TiC-Cu composite particles
International Journal of Refractory Metals and Hard Materials. 2024. V.122. P.106732. DOI: 10.1016/j.ijrmhm.2024.106732 WOS Scopus РИНЦ OpenAlex
Dates:
Submitted: Apr 19, 2024
Accepted: May 17, 2024
Published online: May 19, 2024
Identifiers:
Web of science: WOS:001264359900001
Scopus: 2-s2.0-85193751278
Elibrary: 67335332
OpenAlex: W4397291941
Citing:
DB Citing
OpenAlex 5
Elibrary 5
Scopus 4
Web of science 4
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